Information card for entry 7051864

Structure parameters

• Formula: C95 H134 N6 O2 Pb2
• Calculated formula: C95 H134 N6 O2 Pb2
• Title of publication: Thermally stable lead(ii) amidinates and guanidinates
• Authors of publication: Stasch, Andreas; Forsyth, Craig M.; Jones, Cameron; Junk, Peter C.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2008
• Journal volume: 32
• Journal issue: 5
• Pages of publication: 829
• a: 10.0458 ± 0.0002 Å
• b: 24.5646 ± 0.0006 Å
• c: 17.3771 ± 0.0004 Å
• α: 90°
• β: 97.058 ± 0.001°
• γ: 90°
• Cell volume: 4255.67 ± 0.17 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0915
• Residual factor for significantly intense reflections: 0.0547
• Weighted residual factors for significantly intense reflections: 0.0723
• Weighted residual factors for all reflections included in the refinement: 0.0796
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No