Information card for entry 7051867

Structure parameters

• Formula: C95 H136 Cl2 N6 Pb2
• Calculated formula: C95 H136 Cl2 N6 Pb2
• Title of publication: Thermally stable lead(ii) amidinates and guanidinates
• Authors of publication: Stasch, Andreas; Forsyth, Craig M.; Jones, Cameron; Junk, Peter C.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2008
• Journal volume: 32
• Journal issue: 5
• Pages of publication: 829
• a: 13.2064 ± 0.0003 Å
• b: 13.3847 ± 0.0003 Å
• c: 13.9367 ± 0.0004 Å
• α: 63.026 ± 0.001°
• β: 80.217 ± 0.001°
• γ: 79.878 ± 0.001°
• Cell volume: 2149.88 ± 0.09 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0543
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.0931
• Weighted residual factors for all reflections included in the refinement: 0.0988
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No