Crystallography Open Database

Information card for entry 7052040

7052039 << 7052040 >> 7052041

Preview

Coordinates	7052040.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H45 Ce0.5 Cl N2 Na0.5
Calculated formula	C23 H45 Ce0.5 Cl N2 Na0.5
Title of publication	Cation size dependent reactivity of lanthanide trihalides with bulky alkylcyclopentadienyl anions
Authors of publication	Marc D. Walter; Dirk Bentz; Frank Weber; Oliver Schmitt; Gotthelf Wolmershäuser; Helmut Sitzmann
Journal of publication	New Journal of Chemistry
Year of publication	2007
Journal volume	31
Journal issue	2
Pages of publication	305
a	18.795 ± 0.0009 Å
b	18.795 ± 0.0009 Å
c	29.9286 ± 0.0019 Å
α	90°
β	90°
γ	90°
Cell volume	10572.3 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	88
Hermann-Mauguin space group symbol	I 41/a :2
Hall space group symbol	-I 4ad
Residual factor for all reflections	0.0628
Residual factor for significantly intense reflections	0.0333
Weighted residual factors for significantly intense reflections	0.0715
Weighted residual factors for all reflections included in the refinement	0.0798
Goodness-of-fit parameter for all reflections included in the refinement	0.914
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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