Information card for entry 7052177

Structure parameters

• Formula: C16 H33 Al N2 O
• Calculated formula: C16 H33 Al N2 O
• Title of publication: Synthesis and characterisation of tetramethylpiperidinyloxide (TEMPO) complexes of group 13 metal hydrides
• Authors of publication: Jones, Cameron; Rose, Richard P.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2007
• Journal volume: 31
• Journal issue: 8
• Pages of publication: 1484
• a: 6.35 ± 0.0013 Å
• b: 10.747 ± 0.002 Å
• c: 13.239 ± 0.003 Å
• α: 90°
• β: 92.69 ± 0.03°
• γ: 90°
• Cell volume: 902.5 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.1041
• Residual factor for significantly intense reflections: 0.0679
• Weighted residual factors for significantly intense reflections: 0.1507
• Weighted residual factors for all reflections included in the refinement: 0.1679
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No