Information card for entry 7052179

Structure parameters

• Formula: C25 H50 Al N3 O2
• Calculated formula: C25 H50 Al N3 O2
• SMILES: [AlH](ON1C(CCCC1(C)C)(C)C)(ON1C(CCCC1(C)C)(C)C)[N]12CCC(CC1)CC2
• Title of publication: Synthesis and characterisation of tetramethylpiperidinyloxide (TEMPO) complexes of group 13 metal hydrides
• Authors of publication: Jones, Cameron; Rose, Richard P.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2007
• Journal volume: 31
• Journal issue: 8
• Pages of publication: 1484
• a: 12.707 ± 0.003 Å
• b: 11.963 ± 0.002 Å
• c: 17.66 ± 0.004 Å
• α: 90°
• β: 95.14 ± 0.03°
• γ: 90°
• Cell volume: 2673.8 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.097
• Residual factor for significantly intense reflections: 0.0599
• Weighted residual factors for significantly intense reflections: 0.1197
• Weighted residual factors for all reflections included in the refinement: 0.1356
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No