Information card for entry 7052227

Structure parameters

• Formula: C47 H58 N3 O7 P
• Calculated formula: C47 H58 N3 O7 P
• Title of publication: Structurally diverse penta- and hexacoordinate phosphorus compounds from the reaction of diethyl or diisopropyl azodicarboxylates with phosphorus(iii) compounds
• Authors of publication: Kumar, K. V. P. Pavan; Kumar, N. Satish; Kumara Swamy, K. C.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2006
• Journal volume: 30
• Journal issue: 5
• Pages of publication: 717
• a: 16.7166 ± 0.0011 Å
• b: 15.0867 ± 0.0019 Å
• c: 19.0574 ± 0.0014 Å
• α: 90°
• β: 106.401 ± 0.013°
• γ: 90°
• Cell volume: 4610.7 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2268
• Residual factor for significantly intense reflections: 0.0724
• Weighted residual factors for significantly intense reflections: 0.1616
• Weighted residual factors for all reflections included in the refinement: 0.2228
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No