Highly peri-, regio- and diastereoselective 1,3-dipolar cycloaddition of mesitonitrile oxide to 1,7-dimethyl-2,3-dihydro-1H-1,4-diazepines: unexpected one-step formation of a new triheterocyclic framework
Authors of publication
Baouid, Abdesselam; Elhazazi, Saïd; Hasnaoui, Aïssa; Compain, Philippe; Lavergne, Jean-Pierre; Huet, François
Journal of publication
New Journal of Chemistry
Year of publication
2001
Journal volume
25
Journal issue
12
Pages of publication
1479 - 1481
a
22.9235 ± 0.0007 Å
b
9.9309 ± 0.0005 Å
c
12.8363 ± 0.0007 Å
α
90 ± 0.01°
β
101.078 ± 0.003°
γ
90 ± 0.01°
Cell volume
2867.7 ± 0.2 Å3
Cell temperature
298 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for significantly intense reflections
0.073
Weighted residual factors for all reflections included in the refinement
0.083
Goodness-of-fit parameter for all reflections included in the refinement
