Crystallography Open Database

Information card for entry 7052501

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Coordinates	7052501.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H36 Cl2 N2 O17 P4 Pb3
Calculated formula	C18 H26 Cl2 N2 O17 P4 Pb3
Title of publication	Hydrothermal synthesis, characterization and crystal structures of two new layered lead(ii) diphosphonates
Authors of publication	Sun, Zhong-Ming; Mao, Jiang-Gao; Sun, Yan-Qiong; Zeng, Hui-Yi; Clearfield, Abraham
Journal of publication	New Journal of Chemistry
Year of publication	2003
Journal volume	27
Journal issue	9
Pages of publication	1326
a	9.8986 ± 0.0002 Å
b	31.4972 ± 0.0004 Å
c	10.9253 ± 0.0004 Å
α	90°
β	95.29 ± 0.001°
γ	90°
Cell volume	3391.76 ± 0.15 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	I 1 2/a 1
Hall space group symbol	-I 2ya
Residual factor for all reflections	0.0623
Residual factor for significantly intense reflections	0.0548
Weighted residual factors for significantly intense reflections	0.1519
Weighted residual factors for all reflections included in the refinement	0.1616
Goodness-of-fit parameter for all reflections included in the refinement	1.073
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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