Information card for entry 7052679

Structure parameters

• Formula: C56 H39 B F24 N7 Rh
• Calculated formula: C56 H39 B F24 N7 Rh
• Title of publication: Rhodium(i) complexes bearing N-donor ligands: catalytic activity towards intramolecular cyclization of alkynoic acids and ligand lability
• Authors of publication: Man, Bradley Y.-W.; Bhadbhade, Mohan; Messerle, Barbara A.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2011
• Journal volume: 35
• Journal issue: 8
• Pages of publication: 1730
• a: 12.7104 ± 0.0005 Å
• b: 12.8002 ± 0.0005 Å
• c: 18.2119 ± 0.0007 Å
• α: 80.389 ± 0.002°
• β: 74.396 ± 0.002°
• γ: 81.914 ± 0.002°
• Cell volume: 2799.4 ± 0.19 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0643
• Residual factor for significantly intense reflections: 0.0608
• Weighted residual factors for significantly intense reflections: 0.1511
• Weighted residual factors for all reflections included in the refinement: 0.1534
• Goodness-of-fit parameter for all reflections included in the refinement: 2.732
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No