Information card for entry 7052683

Structure parameters

• Formula: C55 H35 B F24 N7 Rh
• Calculated formula: C55 H35 B F24 N7 Rh
• Title of publication: Rhodium(i) complexes bearing N-donor ligands: catalytic activity towards intramolecular cyclization of alkynoic acids and ligand lability
• Authors of publication: Man, Bradley Y.-W.; Bhadbhade, Mohan; Messerle, Barbara A.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2011
• Journal volume: 35
• Journal issue: 8
• Pages of publication: 1730
• a: 12.6013 ± 0.0008 Å
• b: 12.8203 ± 0.0008 Å
• c: 18.6347 ± 0.0012 Å
• α: 76.517 ± 0.003°
• β: 70.71 ± 0.003°
• γ: 81.166 ± 0.003°
• Cell volume: 2753.5 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1292
• Residual factor for significantly intense reflections: 0.0753
• Weighted residual factors for significantly intense reflections: 0.189
• Weighted residual factors for all reflections included in the refinement: 0.2188
• Goodness-of-fit parameter for all reflections included in the refinement: 1.25
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No