Information card for entry 7053083

Structure parameters

• Formula: Co H48 K4 O62 Si W11
• Calculated formula: Co0.96 K4 O62 Si W11.04
• Title of publication: Mono-substituted silicotungstates as active catalysts for sustainable oxidations: homo- and heterogeneous performance
• Authors of publication: Balula, Salete S.; Cunha-Silva, Luís; Santos, Isabel C. M. S.; Estrada, Ana C.; Fernandes, A. C.; Cavaleiro, José A. S.; Pires, João; Freire, Cristina; Cavaleiro, Ana M. V.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2013
• Journal volume: 37
• Journal issue: 8
• Pages of publication: 2341
• a: 14.1182 ± 0.0007 Å
• b: 14.1182 ± 0.0007 Å
• c: 12.4604 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2483.7 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 128
• Hermann-Mauguin space group symbol: P 4/m n c
• Hall space group symbol: -P 4 2n
• Residual factor for all reflections: 0.0409
• Residual factor for significantly intense reflections: 0.0382
• Weighted residual factors for significantly intense reflections: 0.0952
• Weighted residual factors for all reflections included in the refinement: 0.0971
• Goodness-of-fit parameter for all reflections included in the refinement: 1.15
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No