Crystallography Open Database

Information card for entry 7053460

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Coordinates	7053460.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H59 Al Ge Si4
Calculated formula	C42 H59 Al Ge Si4
Title of publication	Hydroalumination of dialkynylgermanes—synthesis of alkenyl‒alkynylgermanes with intramolecular aluminium‒carbon interactions
Authors of publication	Uhl, Werner; Rohling, Martina; Kösters, Jutta
Journal of publication	New Journal of Chemistry
Year of publication	2010
Journal volume	34
Journal issue	8
Pages of publication	1630
a	11.8818 ± 0.0002 Å
b	17.637 ± 0.0003 Å
c	23.273 ± 0.0003 Å
α	74.141 ± 0.001°
β	81.102 ± 0.001°
γ	79.039 ± 0.001°
Cell volume	4578.53 ± 0.13 Å³
Cell temperature	243 ± 2 K
Ambient diffraction temperature	243 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0886
Residual factor for significantly intense reflections	0.076
Weighted residual factors for significantly intense reflections	0.199
Weighted residual factors for all reflections included in the refinement	0.2104
Goodness-of-fit parameter for all reflections included in the refinement	1.24
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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