Crystallography Open Database

Information card for entry 7053502

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Coordinates	7053502.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H98 Cr2 N10 O2
Calculated formula	C66 H98 Cr2 N10 O2
Title of publication	Reductive N‒N bond cleavage and coupling of organic azides mediated by chromium(i) and vanadium(i) β-diketiminate
Authors of publication	Lin, Kuan-Ming; Wang, Po-Yang; Shieh, Yun-Jen; Chen, Hong-Zhang; Kuo, Ting-Shen; Tsai, Yi-Chou
Journal of publication	New Journal of Chemistry
Year of publication	2010
Journal volume	34
Journal issue	8
Pages of publication	1737
a	12.555 ± 0.0002 Å
b	15.352 ± 0.0002 Å
c	20.174 ± 0.0004 Å
α	75.303 ± 0.001°
β	74.156 ± 0.001°
γ	67.192 ± 0.001°
Cell volume	3399.93 ± 0.1 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1157
Residual factor for significantly intense reflections	0.0907
Weighted residual factors for significantly intense reflections	0.2529
Weighted residual factors for all reflections included in the refinement	0.2796
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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