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Information card for entry 7053506
Preview
Coordinates | 7053506.cif |
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Original paper (by DOI) | HTML |
Formula | C35 H59 Cr N3 Si2 |
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Calculated formula | C35 H59 Cr N3 Si2 |
SMILES | c1(c(C(C)C)cccc1C(C)C)[N]1=C(C)C=C(C)N([Cr]1N([Si](C)(C)C)[Si](C)(C)C)c1c(C(C)C)cccc1C(C)C |
Title of publication | Reductive N‒N bond cleavage and coupling of organic azides mediated by chromium(i) and vanadium(i) β-diketiminate |
Authors of publication | Lin, Kuan-Ming; Wang, Po-Yang; Shieh, Yun-Jen; Chen, Hong-Zhang; Kuo, Ting-Shen; Tsai, Yi-Chou |
Journal of publication | New Journal of Chemistry |
Year of publication | 2010 |
Journal volume | 34 |
Journal issue | 8 |
Pages of publication | 1737 |
a | 9.1132 ± 0.0009 Å |
b | 20.144 ± 0.002 Å |
c | 20.551 ± 0.002 Å |
α | 90° |
β | 90.35 ± 0.002° |
γ | 90° |
Cell volume | 3772.6 ± 0.6 Å3 |
Cell temperature | 200 ± 2 K |
Ambient diffraction temperature | 200 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0767 |
Residual factor for significantly intense reflections | 0.0537 |
Weighted residual factors for significantly intense reflections | 0.1476 |
Weighted residual factors for all reflections included in the refinement | 0.1685 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.052 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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