Information card for entry 7053711

Structure parameters

• Formula: C22 H53 N3 O2.5 Os P2 Si2
• Calculated formula: C22 H53 N3 O2.5 Os P2 Si2
• Title of publication: Reactivity of ?NO with an osmium polyhydride: Reductive elimination and reductive nitrosylation on the path from odd- to even-electron molecules
• Authors of publication: Lee, Joo-Ho; Fan, Hongjun; Pink, Maren; Caulton, Kenneth G.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2007
• Journal volume: 31
• Journal issue: 6
• Pages of publication: 838
• a: 23.2509 ± 0.0016 Å
• b: 23.2509 ± 0.0016 Å
• c: 11.492 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6212.6 ± 1.1 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 7
• Space group number: 114
• Hermann-Mauguin space group symbol: P -4 21 c
• Hall space group symbol: P -4 2n
• Residual factor for all reflections: 0.0331
• Residual factor for significantly intense reflections: 0.0252
• Weighted residual factors for significantly intense reflections: 0.0593
• Weighted residual factors for all reflections included in the refinement: 0.0631
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No