Information card for entry 7054201

Structure parameters

• Chemical name: [Pd12(TePh)24].2DMF
• Formula: C75 H67 N O Pd6 Te12
• Calculated formula: C75 H67 N O Pd6 Te12
• Title of publication: Synthesis, crystal structure, and optical characteristics of [Pd2Hg4Cl6{Te(DMB)}6]·2DMF, [HgClTe(DMB)]4, and the ring-forming cluster [Pd12(TePh)24]·2DMF
• Authors of publication: Tirloni, Barbara; Lang, Ernesto Schulz; de Oliveira, Gelson Manzoni; Piquini, Paulo; Hörner, Manfredo
• Journal of publication: New Journal of Chemistry
• Year of publication: 2014
• Journal volume: 38
• Journal issue: 6
• Pages of publication: 2394
• a: 35.392 ± 0.003 Å
• b: 19.4685 ± 0.0017 Å
• c: 25.583 ± 0.002 Å
• α: 90°
• β: 92.237 ± 0.006°
• γ: 90°
• Cell volume: 17614 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1618
• Residual factor for significantly intense reflections: 0.075
• Weighted residual factors for significantly intense reflections: 0.1662
• Weighted residual factors for all reflections included in the refinement: 0.2025
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No