Halogen-bonded tris(2,4-bis(trichloromethyl)-1,3,5-triazapentadienato)-M(iii) [M = Mn, Fe, Co] complexes and their catalytic activity in the peroxidative oxidation of 1-phenylethanol to acetophenone
Authors of publication
Shixaliyev, Namiq Q.; Gurbanov, Atash V.; Maharramov, Abel M.; Mahmudov, Kamran T.; Kopylovich, Maximilian N.; Martins, Luísa M. D. R. S.; Muzalevskiy, Vasily M.; Nenajdenko, Valentine G.; Pombeiro, Armando J. L.
Journal of publication
New J. Chem.
Year of publication
2014
Journal volume
38
Journal issue
10
Pages of publication
4807
a
10.171 ± 0.003 Å
b
13.499 ± 0.004 Å
c
16.468 ± 0.005 Å
α
79.309 ± 0.006°
β
76.007 ± 0.006°
γ
74.967 ± 0.006°
Cell volume
2100.6 ± 1.1 Å3
Cell temperature
296 ± 2 K
Ambient diffraction temperature
296 ± 2 K
Number of distinct elements
7
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1234
Residual factor for significantly intense reflections
0.077
Weighted residual factors for significantly intense reflections
0.1981
Weighted residual factors for all reflections included in the refinement
0.2395
Goodness-of-fit parameter for all reflections included in the refinement
