Information card for entry 7054342

Structure parameters

• Common name: Bis(n-tetrabutylammonium)bis(tribenzonitrilesilver)decatungstate
• Chemical name: Bis(n-tetrabutylammonium)bis(tribenzonitrilesilver)di-mu5-oxo -icosa-mu-oxo-decaoxodecatungstate
• Formula: C74 H102 Ag2 N8 O32 W10
• Calculated formula: C74 H102 Ag2 N8 O32 W10
• Title of publication: Organoamine silver(i) decatungstate structures: remarkable chemoselectivity and the exploration of the intramolecular redox reaction upon thermolysis
• Authors of publication: Kulikov, Vladislav; Meyer, Gerd
• Journal of publication: New Journal of Chemistry
• Year of publication: 2014
• Journal volume: 38
• Journal issue: 8
• Pages of publication: 3408
• a: 16.0555 ± 0.0006 Å
• b: 24.2744 ± 0.0009 Å
• c: 25.2143 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9827 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.062
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.1177
• Weighted residual factors for all reflections included in the refinement: 0.1291
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No