Crystallography Open Database

Information card for entry 7054947

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Coordinates	7054947.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C88 H148 N6 O9 Si4 Sm2
Calculated formula	C88 H148 N6 O9 Si4 Sm2
Title of publication	Synthesis and characterization of bis(amidate) rare-earth metal amides and their application in catalytic addition of amines to carbodiimides
Authors of publication	Cheng, Hao; Xiao, Yang; Lu, Chengrong; Zhao, Bei; Wang, Yaorong; Yao, Yingming
Journal of publication	New J. Chem.
Year of publication	2015
Journal volume	39
Journal issue	10
Pages of publication	7667
a	13.7002 ± 0.0006 Å
b	13.9301 ± 0.0008 Å
c	15.2548 ± 0.0005 Å
α	108.998 ± 0.004°
β	106.363 ± 0.004°
γ	97.835 ± 0.004°
Cell volume	2556.4 ± 0.2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0432
Residual factor for significantly intense reflections	0.0349
Weighted residual factors for significantly intense reflections	0.0979
Weighted residual factors for all reflections included in the refinement	0.1012
Goodness-of-fit parameter for all reflections included in the refinement	1.128
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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