Information card for entry 7054958

Structure parameters

• Formula: C26 H48 N7 S Sc Si4
• Calculated formula: C26.002 H48.0057 N7 S Sc Si4.001
• Title of publication: Synthesis and structural characterization of amido heteroscorpionate rare-earth metal complexes and hydroamination of aminoalkenes
• Authors of publication: Otero, Antonio; Lara-Sánchez, Agustín; Castro-Osma, José A.; Márquez-Segovia, Isabel; Alonso-Moreno, Carlos; Fernández-Baeza, Juan; Sánchez-Barba, Luis F.; Rodríguez, Ana M.
• Journal of publication: New J. Chem.
• Year of publication: 2015
• Journal volume: 39
• Journal issue: 10
• Pages of publication: 7672
• a: 37.191 ± 0.005 Å
• b: 10.591 ± 0.004 Å
• c: 25.678 ± 0.003 Å
• α: 90°
• β: 133.522 ± 0.012°
• γ: 90°
• Cell volume: 7334 ± 3 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.2141
• Residual factor for significantly intense reflections: 0.0621
• Weighted residual factors for significantly intense reflections: 0.1071
• Weighted residual factors for all reflections included in the refinement: 0.1492
• Goodness-of-fit parameter for all reflections included in the refinement: 0.871
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No