Information card for entry 7055620

Structure parameters

• Formula: C28 H26 N7 Ni O15 Tb
• Calculated formula: C28 H26 N7 Ni O15 Tb
• Title of publication: Nine self-assembled nickel(ii)‒lanthanide(iii) heterometallic complexes constructed from a Salamo-type bisoxime and bearing a N- or O-donor auxiliary ligand: syntheses, structures and magnetic properties
• Authors of publication: Dong, Wen-Kui; Ma, Jian-Chun; Zhu, Li-Chun; Zhang, Yang
• Journal of publication: New J. Chem.
• Year of publication: 2016
• Journal volume: 40
• Journal issue: 8
• Pages of publication: 6998
• a: 10.2398 ± 0.0004 Å
• b: 20.6747 ± 0.0007 Å
• c: 15.2449 ± 0.0005 Å
• α: 90°
• β: 92.096 ± 0.003°
• γ: 90°
• Cell volume: 3225.3 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0419
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.1026
• Weighted residual factors for all reflections included in the refinement: 0.1038
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No