Information card for entry 7055654

Structure parameters

• Formula: C30 H92 Mo12 N10 Ni O73 P8
• Calculated formula: C30 H64 Mo12 N10 Ni O73 P8
• Title of publication: Hydrothermal synthesis of two supramolecular inorganic‒organic hybrid phosphomolybdates based on Ni(ii) and Co(ii) ions: structural diversity and heterogeneous catalytic activities
• Authors of publication: Paul, Luna; Dolai, Malay; Panja, Anangamohan; Ali, Mahammad
• Journal of publication: New J. Chem.
• Year of publication: 2016
• Journal volume: 40
• Journal issue: 8
• Pages of publication: 6931
• a: 13.244 ± 0.005 Å
• b: 13.546 ± 0.005 Å
• c: 14.691 ± 0.005 Å
• α: 74.1 ± 0.005°
• β: 69.748 ± 0.005°
• γ: 65.588 ± 0.005°
• Cell volume: 2225 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0341
• Residual factor for significantly intense reflections: 0.0318
• Weighted residual factors for significantly intense reflections: 0.0896
• Weighted residual factors for all reflections included in the refinement: 0.0912
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No