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Information card for entry 7055771
Preview
Coordinates | 7055771.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C32 H43 I2 N5 |
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Calculated formula | C32 H43 I2 N5 |
Title of publication | Optimised synthesis of monoanionic bis(NHC)-pincer ligand precursors and their Li-complexes |
Authors of publication | Jürgens, Eva; Buys, Kai N.; Schmidt, Anna-Theresa; Furfari, Samantha K.; Cole, Marcus L.; Moser, Michael; Rominger, Frank; Kunz, Doris |
Journal of publication | New J. Chem. |
Year of publication | 2016 |
Journal volume | 40 |
Journal issue | 11 |
Pages of publication | 9160 |
a | 11.373 ± 0.006 Å |
b | 18.404 ± 0.01 Å |
c | 23.13 ± 0.012 Å |
α | 69.64 ± 0.02° |
β | 80.26 ± 0.02° |
γ | 76.44 ± 0.02° |
Cell volume | 4392 ± 4 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1517 |
Residual factor for significantly intense reflections | 0.0692 |
Weighted residual factors for significantly intense reflections | 0.2023 |
Weighted residual factors for all reflections included in the refinement | 0.2583 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.952 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7055771.html
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structural data.