Information card for entry 7055874

Structure parameters

• Formula: C26 H44 Cl4 Li N3 O2 Si Zr
• Calculated formula: C26 H44 Cl4 Li N3 O2 Si Zr
• Title of publication: Zirconium complexes based on an ethylene linked amidinate‒amido ligand: synthesis, characterization and ethylene polymerization
• Authors of publication: Li, Wei; Bai, Sheng-Di; Su, Feng; Yuan, Shi-Fang; Duan, Xin-E; Liu, Dian-Sheng
• Journal of publication: New J. Chem.
• Year of publication: 2017
• Journal volume: 41
• Journal issue: 2
• Pages of publication: 661
• a: 10.584 ± 0.003 Å
• b: 35.281 ± 0.008 Å
• c: 9.826 ± 0.002 Å
• α: 90°
• β: 101.664 ± 0.005°
• γ: 90°
• Cell volume: 3593.4 ± 1.5 ų
• Cell temperature: 194 ± 2 K
• Ambient diffraction temperature: 194 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1089
• Residual factor for significantly intense reflections: 0.0647
• Weighted residual factors for significantly intense reflections: 0.123
• Weighted residual factors for all reflections included in the refinement: 0.1385
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No