Information card for entry 7056502

Structure parameters

• Formula: C36 H27 La8 N6 Nb9 O172 Si3 W27
• Calculated formula: C36 H24 La8 N6 Nb9 O178 Si3 W27
• Title of publication: An Unprecedented 3D Architecture Based on Nb/W Mixed-Addendum Polyoxometalate and Lanthanide-Organic Complex: Synthesis, Crystal Structure and Properties
• Authors of publication: Yang, Mei-Si; Chen, Wei-Chao; Qin, Chao; Yao, Wei; Yin, Ying-Xue; Su, Zhong-Min
• Journal of publication: New J. Chem.
• Year of publication: 2017
• Journal volume: 41
• Journal issue: 19
• Pages of publication: 10532 - 10536
• a: 23.4764 ± 0.0007 Å
• b: 23.4764 ± 0.0007 Å
• c: 12.156 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5802.1 ± 0.4 ų
• Cell temperature: 296 K
• Ambient diffraction temperature: 296 K
• Number of distinct elements: 8
• Space group number: 147
• Hermann-Mauguin space group symbol: P -3
• Hall space group symbol: -P 3
• Residual factor for all reflections: 0.0739
• Residual factor for significantly intense reflections: 0.0615
• Weighted residual factors for significantly intense reflections: 0.1436
• Weighted residual factors for all reflections included in the refinement: 0.1497
• Goodness-of-fit parameter for all reflections included in the refinement: 1.08
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Diffraction radiation X-ray symbol: K-L~3~
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No