Information card for entry 7056593

Structure parameters

• Formula: C28 H28 Mo12 N8 O40 Si
• Calculated formula: C28 H28 Mo12 N8 O40 Si
• Title of publication: Synthesis and photo-/electro-catalytic properties of Keggin polyoxometalate inorganic-organic hybrid layers based on d10 metal and rigid benzo-diazole/-triazole ligands
• Authors of publication: Cao, Yue; Lv, Jinghua; Yu, Kai; Wang, Chunmei; Su, Zhanhua; Wang, Lu; Zhou, Baibin
• Journal of publication: New J. Chem.
• Year of publication: 2017
• Journal volume: 41
• Journal issue: 21
• Pages of publication: 12459 - 12469
• a: 9.9145 ± 0.0016 Å
• b: 11.2727 ± 0.0019 Å
• c: 13.766 ± 0.002 Å
• α: 69.701 ± 0.003°
• β: 82.052 ± 0.003°
• γ: 71.665 ± 0.002°
• Cell volume: 1369 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0858
• Residual factor for significantly intense reflections: 0.0722
• Weighted residual factors for significantly intense reflections: 0.1226
• Weighted residual factors for all reflections included in the refinement: 0.1032
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 0.71068 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No