Information card for entry 7057609

Structure parameters

• Formula: C66 H82 Au B2 K N18
• Calculated formula: C66 H82 Au B2 K N18
• Title of publication: Synthesis and characterization of a gold(i) bis(triazolylidene) complex featuring a large [(TpMe2)2K] anion
• Authors of publication: Priante-Flores, Armando; Salazar-Pereda, Verónica; Rheingold, Arnold L.; Mendoza-Espinosa, Daniel
• Journal of publication: New Journal of Chemistry
• Year of publication: 2018
• Journal volume: 42
• Journal issue: 19
• Pages of publication: 15533
• a: 14.1732 ± 0.0003 Å
• b: 15.601 ± 0.0003 Å
• c: 19.7007 ± 0.0005 Å
• α: 76.639 ± 0.002°
• β: 73.137 ± 0.002°
• γ: 89.372 ± 0.002°
• Cell volume: 4048.63 ± 0.17 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0455
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.1046
• Weighted residual factors for all reflections included in the refinement: 0.1089
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No