Crystallography Open Database

Information card for entry 7057764

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Coordinates	7057764.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C210 H196 Cl4 N24 O60 Tb8
Calculated formula	C210 H196 Cl4 N24 O60 Tb8
Title of publication	Self-assembly of rare octanuclear quad(double-stranded) cluster helicates showing slow magnetic relaxation and the magnetocaloric effect
Authors of publication	Yao, Min-Xia; Cai, Li-Zheng; Deng, Xiao-Wei; Zhang, Wei; Liu, Sui-Jun; Cai, Xu-Min
Journal of publication	New Journal of Chemistry
Year of publication	2018
Journal volume	42
Journal issue	21
Pages of publication	17652
a	18.6643 ± 0.0015 Å
b	20.4817 ± 0.0015 Å
c	34.2977 ± 0.0018 Å
α	83.69 ± 0.002°
β	75.612 ± 0.003°
γ	67.783 ± 0.002°
Cell volume	11755.3 ± 1.4 Å³
Cell temperature	157 ± 2 K
Ambient diffraction temperature	157 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.065
Residual factor for significantly intense reflections	0.0328
Weighted residual factors for significantly intense reflections	0.08
Weighted residual factors for all reflections included in the refinement	0.0845
Goodness-of-fit parameter for all reflections included in the refinement	0.843
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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