Crystallography Open Database

Information card for entry 7057766

Preview

Coordinates	7057766.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C210 H196 Cl4 Ho8 N24 O60
Calculated formula	C210 H196 Cl4 Ho8 N24 O60
Title of publication	Self-assembly of rare octanuclear quad(double-stranded) cluster helicates showing slow magnetic relaxation and the magnetocaloric effect
Authors of publication	Yao, Min-Xia; Cai, Li-Zheng; Deng, Xiao-Wei; Zhang, Wei; Liu, Sui-Jun; Cai, Xu-Min
Journal of publication	New Journal of Chemistry
Year of publication	2018
Journal volume	42
Journal issue	21
Pages of publication	17652
a	18.75 ± 0.002 Å
b	20.5094 ± 0.0011 Å
c	34.3155 ± 0.0017 Å
α	84.101 ± 0.001°
β	75.575 ± 0.002°
γ	67.709 ± 0.001°
Cell volume	11824.5 ± 1.5 Å³
Cell temperature	157 ± 2 K
Ambient diffraction temperature	157 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0747
Residual factor for significantly intense reflections	0.0441
Weighted residual factors for significantly intense reflections	0.1145
Weighted residual factors for all reflections included in the refinement	0.1201
Goodness-of-fit parameter for all reflections included in the refinement	0.933
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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