Information card for entry 7057882

Structure parameters

• Formula: C31 H41 Cl O P2 Ru Si
• Calculated formula: C31 H41 Cl O P2 Ru Si
• Title of publication: Two isomers of a bis(diphenylphosphino)phosphinine, and the synthesis and reactivity of Ru arene/Cp* phosphinophosphinine complexes
• Authors of publication: Newland, Robert J.; Delve, Matthew P.; Wingad, Richard L.; Mansell, Stephen M.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2018
• Journal volume: 42
• Journal issue: 24
• Pages of publication: 19625
• a: 14.6758 ± 0.0005 Å
• b: 14.7658 ± 0.0004 Å
• c: 15.2176 ± 0.0003 Å
• α: 92.281 ± 0.002°
• β: 105.461 ± 0.002°
• γ: 101.298 ± 0.002°
• Cell volume: 3101.92 ± 0.15 ų
• Cell temperature: 120.01 ± 0.1 K
• Ambient diffraction temperature: 120.01 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.0516
• Weighted residual factors for significantly intense reflections: 0.1277
• Weighted residual factors for all reflections included in the refinement: 0.1358
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No