Information card for entry 7057885

Structure parameters

• Formula: C31 H38 Cl4 P2 Ru2 Si
• Calculated formula: C31 H38 Cl4 P2 Ru2 Si
• Title of publication: Two isomers of a bis(diphenylphosphino)phosphinine, and the synthesis and reactivity of Ru arene/Cp* phosphinophosphinine complexes
• Authors of publication: Newland, Robert J.; Delve, Matthew P.; Wingad, Richard L.; Mansell, Stephen M.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2018
• Journal volume: 42
• Journal issue: 24
• Pages of publication: 19625
• a: 9.8194 ± 0.0005 Å
• b: 10.9184 ± 0.0006 Å
• c: 16.7816 ± 0.0009 Å
• α: 99.502 ± 0.003°
• β: 94.824 ± 0.003°
• γ: 105.119 ± 0.003°
• Cell volume: 1697.74 ± 0.16 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.0308
• Weighted residual factors for significantly intense reflections: 0.0618
• Weighted residual factors for all reflections included in the refinement: 0.0659
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No