Information card for entry 7057991

Structure parameters

• Formula: C24 H22 O Si2
• Calculated formula: C24 H22 O Si2
• Title of publication: Catalytic oxidation of diorganosilanes to 1,1,3,3-tetraorganodisiloxanes with gold nanoparticle assembly at the water‒chloroform interface
• Authors of publication: Shankar, Ravi; Sharma, Asmita; Jangir, Bhawana; Chaudhary, Manchal; Kociok-Köhn, Gabriele
• Journal of publication: New Journal of Chemistry
• Year of publication: 2019
• Journal volume: 43
• Journal issue: 2
• Pages of publication: 813
• a: 12.567 ± 0.007 Å
• b: 6.088 ± 0.004 Å
• c: 14.018 ± 0.008 Å
• α: 90°
• β: 95.794 ± 0.016°
• γ: 90°
• Cell volume: 1067 ± 1.1 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0749
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.12
• Weighted residual factors for all reflections included in the refinement: 0.1428
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No