Information card for entry 7058192

Structure parameters

• Formula: C48 H40 Cl10 Fe2 O2 P2 Pd2
• Calculated formula: C48 H40 Cl10 Fe2 O2 P2 Pd2
• Title of publication: Synthesis and characterisation of palladium(ii) complexes with hybrid phosphinoferrocene ligands bearing additional O-donor substituents
• Authors of publication: Vosáhlo, Petr; Schulz, Jiří; Škoch, Karel; Císařová, Ivana; Štěpnička, Petr
• Journal of publication: New Journal of Chemistry
• Year of publication: 2019
• Journal volume: 43
• Journal issue: 11
• Pages of publication: 4463
• a: 14.6498 ± 0.0003 Å
• b: 9.3791 ± 0.0002 Å
• c: 18.883 ± 0.0003 Å
• α: 90°
• β: 92.328 ± 0.001°
• γ: 90°
• Cell volume: 2592.42 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0215
• Residual factor for significantly intense reflections: 0.0187
• Weighted residual factors for significantly intense reflections: 0.0441
• Weighted residual factors for all reflections included in the refinement: 0.0452
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No