Information card for entry 7058340

Structure parameters

• Formula: C14 H13 Cl2 Fe N3 O4
• Calculated formula: C14 H14 Cl2 Fe N3 O4
• Title of publication: Distinct supramolecular assemblies of Fe(iii) and Ni(ii) complexes constructed from the o-vanillin salicylhydrazone ligand: syntheses, crystal structures, DNA/protein interaction, and antioxidant and cytotoxic activity
• Authors of publication: Li, Yueqin; Li, Yun; Yang, Zhiwei; Meng, Fantao; Wang, Nana; Zhou, Minya; Xia, Zongbiao; Gong, Qiang; Gao, Qinwei
• Journal of publication: New Journal of Chemistry
• Year of publication: 2019
• Journal volume: 43
• Journal issue: 21
• Pages of publication: 8024
• a: 8.177 ± 0.003 Å
• b: 22.891 ± 0.007 Å
• c: 10.113 ± 0.002 Å
• α: 90°
• β: 117.87 ± 0.02°
• γ: 90°
• Cell volume: 1673.4 ± 0.9 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0587
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.1034
• Weighted residual factors for all reflections included in the refinement: 0.1219
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No