Information card for entry 7058439

Structure parameters

• Formula: C48 H75 N2 P Th
• Calculated formula: C48 H75 N2 P Th
• Title of publication: Preparation of a potassium chloride bridged thorium phosphinidiide complex and its reactivity towards small organic molecules
• Authors of publication: Wang, Yongsong; Zhang, Congcong; Zi, Guofu; Ding, Wanjian; Walter, Marc D.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2019
• Journal volume: 43
• Journal issue: 24
• Pages of publication: 9527
• a: 10.6048 ± 0.0007 Å
• b: 14.0877 ± 0.0011 Å
• c: 17.0948 ± 0.0011 Å
• α: 79.425 ± 0.006°
• β: 88.351 ± 0.005°
• γ: 70.872 ± 0.006°
• Cell volume: 2370.6 ± 0.3 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0701
• Residual factor for significantly intense reflections: 0.0556
• Weighted residual factors for significantly intense reflections: 0.1122
• Weighted residual factors for all reflections included in the refinement: 0.1198
• Goodness-of-fit parameter for all reflections included in the refinement: 1.089
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No