Information card for entry 7058442

Structure parameters

• Formula: C96 H140 Cl2 K2 N2 P2 Th2
• Calculated formula: C96 H140 Cl2 K2 N2 P2 Th2
• Title of publication: Preparation of a potassium chloride bridged thorium phosphinidiide complex and its reactivity towards small organic molecules
• Authors of publication: Wang, Yongsong; Zhang, Congcong; Zi, Guofu; Ding, Wanjian; Walter, Marc D.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2019
• Journal volume: 43
• Journal issue: 24
• Pages of publication: 9527
• a: 24.8824 ± 0.0006 Å
• b: 11.6832 ± 0.0003 Å
• c: 32.2158 ± 0.0007 Å
• α: 90°
• β: 92.277 ± 0.002°
• γ: 90°
• Cell volume: 9357.9 ± 0.4 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0617
• Residual factor for significantly intense reflections: 0.0443
• Weighted residual factors for significantly intense reflections: 0.0928
• Weighted residual factors for all reflections included in the refinement: 0.1006
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No