Unexpected intramolecular N-arylcyano-β-diketiminate cyclization in new aminoquinoline derivative complexes of aluminium for CO2 fixation into cyclic carbonates
Authors of publication
Moreno da Costa, David; Borja, Luis; Verdugo, Camilo; Martinez, Javier; Quintero, Celso; Jaque, Pablo; Trofymchuk, Oleksandra S.; Daniliuc, Constantin G.; Cabrera, Alan R.; Rojas, Rene S.
Journal of publication
New Journal of Chemistry
Year of publication
2019
Journal volume
43
Journal issue
30
Pages of publication
12059
a
25.7345 ± 0.0009 Å
b
11.2523 ± 0.0004 Å
c
18.8485 ± 0.0006 Å
α
90°
β
124.671 ± 0.002°
γ
90°
Cell volume
4488.8 ± 0.3 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0552
Residual factor for significantly intense reflections
0.0427
Weighted residual factors for significantly intense reflections
0.1087
Weighted residual factors for all reflections included in the refinement
0.1163
Goodness-of-fit parameter for all reflections included in the refinement
