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Information card for entry 7059165
Preview
Coordinates | 7059165.cif |
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Original paper (by DOI) | HTML |
Formula | C62 H68 Br6 N10 Ni3 P2 |
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Calculated formula | C62 H68 Br6 N10 Ni3 P2 |
Title of publication | Catalytic systems based on nickel(ii) complexes with bis(3,5-dimethylpyrazol-1-yl)methane ‒ impact of PPh3 on the formation of precatalysts and selective dimerization of ethylene |
Authors of publication | Zubkevich, S. V.; Tuskaev, V. A.; Gagieva, S. Ch.; Pavlov, A. A.; Khrustalev, V. N.; Polyakova, O. V.; Zarubin, D. N.; Kurmaev, D. A.; Kolosov, N. A.; Bulychev, B. M. |
Journal of publication | New Journal of Chemistry |
Year of publication | 2020 |
Journal volume | 44 |
Journal issue | 3 |
Pages of publication | 981 - 993 |
a | 9.6743 ± 0.0019 Å |
b | 10.044 ± 0.002 Å |
c | 20.289 ± 0.004 Å |
α | 79.47 ± 0.03° |
β | 76.24 ± 0.03° |
γ | 64.55 ± 0.03° |
Cell volume | 1721.8 ± 0.7 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.141 |
Residual factor for significantly intense reflections | 0.1139 |
Weighted residual factors for significantly intense reflections | 0.2548 |
Weighted residual factors for all reflections included in the refinement | 0.2933 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.808 |
Diffraction radiation wavelength | 0.9699 Å |
Diffraction radiation type | synchrotron |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7059165.html
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