Theoretical and experimental study of the coordination ability of 4,6-dimethylpyrimidinylhydrazone diacetylmonooxime towards Ni(ii), Mn(ii), Fe(iii) and Co(iii) ions
Authors of publication
Lukov, Vladimir V.; Tsaturyan, Arshak A.; Tupolova, Yulia P.; Popov, Leonid D.; Shcherbakov, Igor N.; Lebedev, Vladimir E.; Askalepova, Olga I.; Lastovina, Tatiana A.; Lazarenko, Vladimir A.; Khustalev, Victor N.; Poler, Jordan C.
Journal of publication
New Journal of Chemistry
Year of publication
2020
Journal volume
44
Journal issue
5
Pages of publication
2146 - 2154
a
10.0278 ± 0.0004 Å
b
10.815 ± 0.0004 Å
c
11.265 ± 0.0004 Å
α
90°
β
98.834 ± 0.001°
γ
90°
Cell volume
1207.2 ± 0.08 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
4
Space group number
13
Hermann-Mauguin space group symbol
P 1 2/n 1
Hall space group symbol
-P 2yac
Residual factor for all reflections
0.0769
Residual factor for significantly intense reflections
0.0463
Weighted residual factors for significantly intense reflections
0.1219
Weighted residual factors for all reflections included in the refinement
0.1388
Goodness-of-fit parameter for all reflections included in the refinement
