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Information card for entry 7059700
Preview
Coordinates | 7059700.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C36 H32 Cl F6 Ni O P3 S2 |
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Calculated formula | C36 H32 Cl F6 Ni O P3 S2 |
Title of publication | Synthesis and characterization of new square planar heteroleptic cationic complexes [Ni(ii) β-oxodithioester-dppe]+; their use as a catalyst for Chan‒Lam coupling |
Authors of publication | Kumari, Kavita; Kumar, Saurabh; Singh, Krishna Nand; Drew, Michael G. B.; Singh, Nanhai |
Journal of publication | New Journal of Chemistry |
Year of publication | 2020 |
Journal volume | 44 |
Journal issue | 28 |
Pages of publication | 12143 - 12153 |
a | 11.0392 ± 0.0006 Å |
b | 12.2336 ± 0.0006 Å |
c | 27.2764 ± 0.0015 Å |
α | 90° |
β | 96.775 ± 0.006° |
γ | 90° |
Cell volume | 3657.9 ± 0.3 Å3 |
Cell temperature | 150 ± 2 K |
Ambient diffraction temperature | 150 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1729 |
Residual factor for significantly intense reflections | 0.09 |
Weighted residual factors for significantly intense reflections | 0.1804 |
Weighted residual factors for all reflections included in the refinement | 0.2155 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.994 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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