Information card for entry 7059732

Structure parameters

• Common name: (AsPh4)4[(WO2)4(9HL)4].4MeOH.4H2O
• Formula: C152 H124 As4 O36 W4
• Calculated formula: C150 H108 As4 O30 W4
• Title of publication: A new fluorone-based bridging ligand for discrete and polymeric assemblies including Mo and W based [4+4] metallocycles
• Authors of publication: Sutton, Ashley L.; Abrahams, Brendan F.; Hudson, Timothy A.; Robson, Richard
• Journal of publication: New Journal of Chemistry
• Year of publication: 2020
• Journal volume: 44
• Journal issue: 27
• Pages of publication: 11437 - 11440
• a: 30.3905 ± 0.0003 Å
• b: 30.3905 ± 0.0003 Å
• c: 14.8757 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 13738.9 ± 0.3 ų
• Cell temperature: 130.15 K
• Ambient diffraction temperature: 130.15 K
• Number of distinct elements: 5
• Space group number: 92
• Hermann-Mauguin space group symbol: P 41 21 2
• Hall space group symbol: P 4abw 2nw
• Residual factor for all reflections: 0.0467
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.0964
• Weighted residual factors for all reflections included in the refinement: 0.098
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No