Information card for entry 7061675

Structure parameters

• Formula: C20 H36 O11 Rh2 Si2
• Calculated formula: C20 H36 O11 Rh2 Si2
• Title of publication: Multinuclear rhodium complexes supported by tetra-tert-butoxy disiloxide ligand: synthesis, structure, and reactivity
• Authors of publication: Ishizaka, Yusuke; Matsumoto, Kazuhiro; Sato, Kazuhiko; Choi, Jun-Chul
• Journal of publication: New Journal of Chemistry
• Year of publication: 2022
• Journal volume: 46
• Journal issue: 33
• Pages of publication: 16040 - 16046
• a: 9.3394 ± 0.0002 Å
• b: 11.5662 ± 0.0002 Å
• c: 14.9335 ± 0.0003 Å
• α: 112.248 ± 0.002°
• β: 99.31 ± 0.002°
• γ: 99.762 ± 0.002°
• Cell volume: 1425.56 ± 0.06 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0369
• Residual factor for significantly intense reflections: 0.0281
• Weighted residual factors for significantly intense reflections: 0.0888
• Weighted residual factors for all reflections included in the refinement: 0.0962
• Goodness-of-fit parameter for all reflections included in the refinement: 0.768
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No