Information card for entry 7062158

Structure parameters

• Formula: C88 H60 B Cu F24 N2 P2
• Calculated formula: C88 H60 B Cu F24 N2 P2
• Title of publication: Developing bulky P-alkene ligands: stabilization of copper complexes with 14 valence electrons
• Authors of publication: Grasruck, Alexander; Parla, Giorgio; Heineman, Frank W.; Langer, Jens; Herrera, Alberto; Frieß, Sybille; Schmid, Günter; Dorta, Romano
• Journal of publication: New Journal of Chemistry
• Year of publication: 2023
• Journal volume: 47
• Journal issue: 5
• Pages of publication: 2307 - 2323
• a: 19.862 ± 0.0012 Å
• b: 19.0191 ± 0.0011 Å
• c: 20.6755 ± 0.001 Å
• α: 90°
• β: 95.469 ± 0.002°
• γ: 90°
• Cell volume: 7774.8 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0618
• Residual factor for significantly intense reflections: 0.0396
• Weighted residual factors for significantly intense reflections: 0.0788
• Weighted residual factors for all reflections included in the refinement: 0.0879
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No