Information card for entry 7062176

Structure parameters

• Formula: C99 H94 Cl6 Dy4 N7 O33
• Calculated formula: C99 H94 Cl6 Dy4 N7 O33
• Title of publication: Asymmetric {Dy4} metallogrid and double-layered {Dy8} cage clusters from carboxylic decorated o-vanillin Schiff bases: syntheses, topological variation, and single molecule magnet behaviors
• Authors of publication: Wang, Yi-Han; Qin, Yu; Tang, Shen; Teng, Qing-Hu; Zhu, Meng-Meng; Peng, Song; Wang, Kai; Liang, Fu-Pei
• Journal of publication: New Journal of Chemistry
• Year of publication: 2023
• Journal volume: 47
• Journal issue: 4
• Pages of publication: 2052 - 2059
• a: 29.0219 ± 0.0007 Å
• b: 19.1466 ± 0.0005 Å
• c: 19.2115 ± 0.0005 Å
• α: 90°
• β: 100.539 ± 0.003°
• γ: 90°
• Cell volume: 10495.2 ± 0.5 ų
• Cell temperature: 100.01 K
• Ambient diffraction temperature: 100.01 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1092
• Residual factor for significantly intense reflections: 0.0772
• Weighted residual factors for significantly intense reflections: 0.153
• Weighted residual factors for all reflections included in the refinement: 0.1723
• Goodness-of-fit parameter for all reflections included in the refinement: 1.176
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No