Information card for entry 7062187

Structure parameters

• Formula: C3 H3.4 Cl0.4 N0.2 P0.2 Pd0.2
• Calculated formula: C3 H3.4 Cl0.4 N0.2 P0.2 Pd0.2
• Title of publication: Palladium(ii)-complexes of bi- and tri-dentate phosphine ligands: precursor for palladium–phosphorous nanoparticles and activity towards Suzuki–Miyaura coupling
• Authors of publication: Rao, Gyandshwar Kumar; Dutta, Anirban; Yadav, Nisha; Oswal, Preeti; Kumar, Arun; Singh, Ajai K.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2023
• Journal volume: 47
• Journal issue: 9
• Pages of publication: 4218 - 4227
• a: 34.786 ± 0.01 Å
• b: 12.983 ± 0.004 Å
• c: 17.594 ± 0.005 Å
• α: 90°
• β: 107.457 ± 0.005°
• γ: 90°
• Cell volume: 7580 ± 4 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273.15 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0785
• Residual factor for significantly intense reflections: 0.0589
• Weighted residual factors for significantly intense reflections: 0.1226
• Weighted residual factors for all reflections included in the refinement: 0.1313
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No