Information card for entry 7062359

Structure parameters

• Formula: C12 H24 Cl K O7
• Calculated formula: C12 H24 Cl K O7
• Title of publication: Characterization and isolation of an 18-crown-6 complex of potassium hydroxide prepared by milling: application to mechanochemical organic synthesis
• Authors of publication: Vugrin, Leonarda; Halasz, Ivan; Geneste, Hervé
• Journal of publication: New Journal of Chemistry
• Year of publication: 2023
• Journal volume: 47
• Journal issue: 16
• Pages of publication: 7466 - 7469
• a: 8.06245 ± 0.00077 Å
• b: 13.9387 ± 0.0012 Å
• c: 8.01697 ± 0.00067 Å
• α: 90°
• β: 97.5456 ± 0.0055°
• γ: 90°
• Cell volume: 893.15 ± 0.14 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• RFsqd: 0.0396
• Goodness-of-fit parameter for all reflections: 1.34
• Method of determination: powder diffraction
• Diffraction radiation wavelength: 1.54056 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No