Information card for entry 7062393

Structure parameters

• Formula: C17 H20 Cl2 F3 N O Ru
• Calculated formula: C17 H20 Cl2 F3 N O Ru
• Title of publication: N-coordinated Ru(ii) catalyzed solvent free N-alkylation of primary amines with alcohols through borrowing hydrogen strategy
• Authors of publication: Patel, Bhavya; Ranjan, Rishi; Chauhan, Nimesh R.; Mukhopadhyay, Suman; Choudhury, Angshuman Roy; Vyas, Komal M.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2023
• Journal volume: 47
• Journal issue: 17
• Pages of publication: 8305 - 8317
• a: 7.8494 ± 0.0005 Å
• b: 9.0853 ± 0.0005 Å
• c: 14.9436 ± 0.0009 Å
• α: 81.364 ± 0.005°
• β: 89.73 ± 0.005°
• γ: 70.383 ± 0.005°
• Cell volume: 991.26 ± 0.11 ų
• Cell temperature: 298 ± 0.2 K
• Ambient diffraction temperature: 298 ± 0.2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0929
• Residual factor for significantly intense reflections: 0.0683
• Weighted residual factors for significantly intense reflections: 0.1852
• Weighted residual factors for all reflections included in the refinement: 0.2261
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No