Crystallography Open Database

Information card for entry 7062586

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Coordinates	7062586.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C71 H59.4 Cl8 N4 O0.7 P2 Ru2
Calculated formula	C64 H50 Cl7 N4 P2 Ru2
Title of publication	Di-ruthenium complexes of 1,4-diazabutadiene ligands: synthesis, characterization and utilization as catalyst precursors for the oxidative coupling of amines to imines in air
Authors of publication	Saha, Rumpa; Mukherjee, Aparajita; Bhattacharya, Samaresh
Journal of publication	New Journal of Chemistry
Year of publication	2023
Journal volume	47
Journal issue	27
Pages of publication	12709 - 12717
a	32.926 ± 0.005 Å
b	17.173 ± 0.002 Å
c	26.459 ± 0.003 Å
α	90°
β	113.647 ± 0.004°
γ	90°
Cell volume	13705 ± 3 Å³
Cell temperature	273 ± 2 K
Ambient diffraction temperature	273.15 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1813
Residual factor for significantly intense reflections	0.1066
Weighted residual factors for significantly intense reflections	0.29
Weighted residual factors for all reflections included in the refinement	0.3686
Goodness-of-fit parameter for all reflections included in the refinement	1.1102
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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