Information card for entry 7062840

Structure parameters

• Formula: C32 H28 N4 Ni2 O14
• Calculated formula: C28 H22 N4 Ni2 O10
• Title of publication: Structures and magnetic studies of four new Ni(ii) coordination polymers built using symmetrical tetracarboxylate and N-donor linkers
• Authors of publication: Zhang, Xiaoyu; Qin, Tianrui; Liu, Yichen; An, Ning; Afzal, Mohd; Alarifi, Abdullah; Muddassir, Mohd.; Sakiyama, Hiroshi; Mohanty, Aurobinda; Dong, Xiuyan
• Journal of publication: New Journal of Chemistry
• Year of publication: 2023
• Journal volume: 47
• Journal issue: 46
• Pages of publication: 21214 - 21224
• a: 8.0206 ± 0.0003 Å
• b: 9.7574 ± 0.0003 Å
• c: 13.0392 ± 0.0004 Å
• α: 110.763 ± 0.001°
• β: 90.633 ± 0.002°
• γ: 112.746 ± 0.002°
• Cell volume: 866.89 ± 0.05 ų
• Cell temperature: 190 ± 2 K
• Ambient diffraction temperature: 190 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0998
• Residual factor for significantly intense reflections: 0.0895
• Weighted residual factors for significantly intense reflections: 0.236
• Weighted residual factors for all reflections included in the refinement: 0.2412
• Goodness-of-fit parameter for all reflections included in the refinement: 1.097
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No