Information card for entry 7062917

Structure parameters

• Formula: C35 H30 N P2
• Calculated formula: C35 H30 N P2
• Title of publication: Aryl group transfer and C–P bond formation in the reaction of organonickel complexes with sodium 3,4,5-triphenyl-1,2-diphospholide
• Authors of publication: Sakhapov, I. F.; Zagidullin, A. A.; Gafurov, Z. N.; Khismatova, D. K.; Zaripov, R. B.; Kagilev, A. A.; Kantyukov, A. O.; Zueva, E. M.; Petrova, M. M.; Litvinov, I. A.; Miluykov, V. A.; Shmelev, A. G.; Sinyashin, O. G.; Yakhvarov, D. G.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2024
• Journal volume: 48
• Journal issue: 4
• Pages of publication: 1559 - 1566
• a: 24.277 ± 0.0008 Å
• b: 15.336 ± 0.0006 Å
• c: 17.4979 ± 0.0011 Å
• α: 90°
• β: 119.683 ± 0.001°
• γ: 90°
• Cell volume: 5659.8 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0489
• Residual factor for significantly intense reflections: 0.0385
• Weighted residual factors for significantly intense reflections: 0.0986
• Weighted residual factors for all reflections included in the refinement: 0.1043
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No